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Effect of Alkyl Chain Length of Amines on the Micro-structural and Magnetic Properties of Stabilized Ni-NiO Nanoparticles

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Abstract

Different long-chain primary alkylamines such as octylamine, dodecylamine, tetradecylamine, hexadecylamine or octadecylamine were used to stabilize Ni-NiO nanoparticles (metal:stabilizer ratio of 1:10) by an organometallic method in organic medium to evaluate their effect on the microstructural and magnetic properties. The Ni-NiO stabilized nanoparticles were characterized by Fourier transformed infrared (FT-IR), X-ray photoelectron spectroscopy (XPS), conventional transmission electron microscopy (TEM), high resolution transmission electron microscopy (HRTEM), X-ray diffraction (XRD) and dynamic light scattering (DLS). The results indicated an adequate stabilization of Ni nanoparticles with the different primary alkylamines. The semi-quantitative analysis suggests that Ni surface composition is a combination of the metallic state with NiO, NiOOH and NiO, but the chain length modified the content and proportion of these compounds. The highest Ni metallic state (57.2 at. %) was obtained with tetradecylamine as stabilizer. The morphology of the samples is similar to a core–shell semi-spherical, but the particle size tends to reduce with the alkyl chain length of primary amines from 20 to 8 nm. The saturation magnetization (Ms) showed important variations depending on the surface composition, for which variable particle size and Ni metallic content were determining factors for the magnetic response.

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The datasets generated during and/or analysed during the current study are available from the corresponding author on reasonable request.

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Acknowledgements

The authors wish to acknowledge the financial support provided by Dirección de Investigación-Universidad Iberoamericana through the postdoctoral and INIAT F145021 projects, FICSAC, the Instituto Politécnico Nacional through the SIP2022-0668, -0671, -1153, -1155, and -0244 projects; CONACyT CB2015-252181 and 157613 projects; as well as SNI-CONACyT.

Funding

This study was funded by Universidad Iberoamaericana, Instituto Politécnico Nacional and Consejo Nacional de ciencia y tecnología de México.

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Authors and Affiliations

  1. Departamento de Ingeniería Química, Universidad Iberoamericana, Industrial y de Alimentos, Prolongación Paseo de la Reforma 880, Lomas de Santa Fe, C.P. 01219, Mexico City, México

    L. P. A. Guerrero-Ortega & E. Ramírez-Meneses

  2. Universidad Nacional Autónoma de México Instituto de Investigaciones en Materiales, Ciudad Universitaria, Circuito Exterior s/n, Coyoacán, C.P.04510, Mexico City, México

    I. Betancourt & R. Mendoza-Cruz

  3. Instituto Politécnico Nacional, Centro de Nanociencias y Micro y Nanotecnologías, UPALM Zacatenco, C.P. 07738, Mexico City, Mexico

    L. Lartundo-Rojas

  4. Instituto Politécnico Nacional, UPIIH, San Agustín Tlaxcala, Ciudad Del Conocimiento y La Cultura, Carretera Pachuca-Actopan Km. 1+500, Hidalgo, Mexico

    A. M. Torres-Huerta & M. A. Domínguez-Crespo

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All authors whose names appear on the submission approved the version to be published and agree to be accountable for all aspects of the work in ensuring that questions related to the accuracy or integrity of any part of the work are appropriately investigated and resolved. LPAG-O: conceptualization, methodology, formal analysis. ER-M: conceptualization, methodology, formal analysis, resources, writing—review & editing. IB: supervision, magnetic characterization. LL-R: XPS analyses, revision—original draft. RM-C: characterization-supervision. AMT-H: formal analysis, resources, writing—review & editing, supervision, funding acquisition. MAD-C: conceptualization, writing—original draft, methodology, formal analysis, resources, writing—review & editing.

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Guerrero-Ortega, L.P.A., Ramírez-Meneses, E., Betancourt, I. et al. Effect of Alkyl Chain Length of Amines on the Micro-structural and Magnetic Properties of Stabilized Ni-NiO Nanoparticles. J Inorg Organomet Polym 33, 368–382 (2023). https://doi.org/10.1007/s10904-022-02506-7

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